Florida Regulations 62-160.300: Laboratory Certification
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(1) Except as provided in subsections 62-160.300(2) through (8), F.A.C., all laboratories generating environmental data for submission to the Department or for use in Department-regulated or Department-sponsored activities shall hold certification from the Florida Department of Health, Environmental Laboratory Certification Program (DOH ELCP). Such certification shall be for all matrix/test method/analyte(s) combinations being measured. The matrix of a sample is defined to be the condition under which the laboratory originally receives the sample, and shall be classified according to the Field of Accreditation Matrix groups defined by subsection 62-160.120(18), F.A.C.
(a) Certification shall be based on the matrix of the sample. The matrix of a sample is defined to be the condition under which the laboratory originally receives the sample, and shall be classified according to the Field of Accreditation Matrix groups defined by subsection 62-160.120(18), F.A.C.
(b) For laboratories reporting data for drinking water compliance, certification shall be for all matrix/text method/analyte(s) combinations being reported.
(c) For the non-potable water matrix, laboratories shall apply for and receive DOH ELCP certification in at least one method for each analytical technology/analyte combination being measured. The Department will accept any of the combinations certified by the DOH ELCP, according to Fl. Admin. Code R. 64E-1.102, dated 1-24-05.
1. When a Department contract, order, permit or title 62 rules requires a specific method to be reported, laboratories shall report only that method. Laboratories may report additional analytes not published in the reported method, if the applicable requirements in Fl. Admin. Code R. 62-160.330 are met, and the laboratory is certified according to Fl. Admin. Code R. 62-160.300(1)(c)
2. Except as noted in subFl. Admin. Code R. 62-160.300(1)(c)1., above, laboratories may report results by any method that is equivalent in technology to the method for which they hold certification, provided they are certified according to Fl. Admin. Code R. 62-160.300(1)(c), for the analyte that is reported. When laboratories report a method for which they do not hold certification, the laboratory shall document that all requirements of the reported method are met.
3. If a laboratory is required to provide data for an analyte for which, according to subsection 62-160.320(1), F.A.C., no method is published for the non-potable water matrix, or the published method for the non-potable water matrix does not meet required data quality objectives established by the Department for a project, but a method is published for the drinking water matrix, and the Department has recognized that the published drinking water method meets the data quality objectives for the Department project for which the method will be used according to subsection 62-160.320(1), F.A.C., the laboratory is not required to obtain certification for the analytical technology/analyte combination in the non-potable water matrix. However, the laboratory must be certified in the drinking water matrix for the reported test method/analyte combination.
(d) For all other matrices, laboratories shall apply for and receive certification for all matrix/test method/analyte combinations that are reported to the Department.
(2) To the extent possible, a laboratory must be certified as specified in subsection 62-160.300(1), F.A.C., before reporting results for a given matrix/analytical technology or test method/analyte combination. However, if a laboratory makes a written request to the Department to use a method that is not certified, the Department will allow a laboratory to begin using a method before the certification process is complete if the following requirements are met.
(a) The laboratory must have met all the requirements for certification except for the on-site visit by DOH ELCP inspectors. The laboratory must be prepared to provide to the Department copies of the relevant application, applicable performance test sample results and the initial demonstration of capability.
(b) The precision, accuracy and method detection limits generated by the laboratory must meet or exceed the project specific data quality objectives.
(c) The laboratory shall notify the Department of the status of its certification application within 5 business days of receiving notification by DOH ELCP of the certification granted for the specific matrix/analytical technology or test method/analyte combination requested.
(3) Laboratory certification by the DOH ELCP is not required for the following test procedures identified in subsections 62-550.550(1) and (2), F.A.C., when conducted by an operator licensed under Fl. Admin. Code Chapter 62-602, or by persons under the direct supervision of a licensed operator, for the purposes of drinking water compliance:
(a) Alkalinity;
(b) Bromide;
(c) Calcium;
(d) Chlorite (only at entrances to distribution systems);
(e) Specific conductance;
(f) Disinfectant residual (includes residual chlorine);
(g) Orthophosphate;
(h) pH;
(i) Silica;
(j) Specific ultraviolet absorbance;
(k) Temperature;
(l) Total organic carbon;
(m) Turbidity, or
(n) Any analytes in addition to those listed in paragraphs 62-160.300(3)(a) through 62-160.300(3)(m), F.A.C., above that are exempted from laboratory certification according to subsections 62-550.550(1) and 62-550.550(2), F.A.C., for the specific compliance applications described therein.
(o) The analytes exempted in paragraphs 62-160.300(3)(a) through 62-160.300(3)(n), F.A.C., above shall be analyzed according to all applicable requirements for analyses according to subsections 62-550.550(1) and 62-550.550(2), F.A.C., for the specific compliance applications described therein.
(p) In cases where the Department has a specific field testing method standard operating procedure (e.g., FT 1100 for pH, in DEP-SOP-001/01, which is incorporated by reference in subFl. Admin. Code R. 62-160.800(1)(a)19.), the laboratory or authorized person, as described in Fl. Admin. Code R. 62-550.550, shall follow the Department’s procedures. For all other analytes, a laboratory or authorized person, as described in Fl. Admin. Code R. 62-550.550, shall only use test methods that are acceptable for drinking water compliance, as specified in Fl. Admin. Code R. 62-550.550 and shall follow all requirements for calibration verification according to DEP SOP FT 1000 in DEP-SOP-001/01, which is incorporated by reference in subFl. Admin. Code R. 62-160.800(1)(a)18.
(4) Certification by the DOH ELCP is not required when conducting the test procedures for the analytes listed in paragraphs 62-160.300(4)(a) through (h), F.A.C., because the Department’s standard operating procedures (SOPs) are more stringent than the corresponding laboratory test methods certified by DOH ELCP. When conducting these test procedures, laboratories shall follow the applicable SOPs in DEP-SOP-001/01 (January 2017), which are incorporated by reference in Fl. Admin. Code R. 62-160.800(1)(a)
(a) pH;
(b) Dissolved oxygen;
(c) Specific conductance;
(d) Temperature;
(e) Total residual chlorine (including free available chlorine);
(f) Salinity;
(g) Turbidity; and,
(h) Any other test with a specified holding time of fifteen minutes or less when performed as a field procedure.
(5) Certification is not required for the following tests or analyses:
(a) Any analyses related solely to internal process control, unless the test data are reported to the Department to meet compliance monitoring requirements for a Department-issued permit;
(b) Laboratory tests conducted for research projects, as described in Fl. Admin. Code R. 62-160.600, or
(c) Methods used by statutorily created volunteer monitoring organizations, when the Department has reviewed and concluded that the organization’s Standard Operating Procedures provide sufficient quality assurance requirements for Department purposes.
(6) Certification by the DOH ELCP is not required for methods and procedures required to perform the Specific Oxygen Uptake Rate (SOUR) test, when performed by an operator certified in accordance with Fl. Admin. Code Chapter 62-602, or persons under the direction of a certified operator, as authorized by Fl. Admin. Code Chapter 62-640
(7) Certification is not required for any test in which the reported result is a calculation from the results of other tests for which the laboratory holds certification by the DOH ELCP.
(8) Certification is not required for those matrix/method/analyte combinations (such as taxonomic identification) that are not included in the DOH ELCP scope of accreditation.
(9) If certification is not required (see subsections 62-160.300(3) through (8), F.A.C.), laboratory organizations shall follow the relevant Department-approved methods as provided in Fl. Admin. Code R. 62-160.320, and shall meet all other requirements for laboratories as provided in this chapter.
Rulemaking Authority 403.061, 403.0623, 403.0625, 403.863 FS. Law Implemented 373.026, 373.309, 373.409, 373.413, 373.414, 373.416, 373.4592, 376.303, 376.305, 376.3071, 403.0623, 403.0625, 403.087, 403.088, 403.0881, 403.504, 403.704, 403.707, 403.722, 403.803, 403.853 FS. History-New 1-1-91, Amended 2-4-93, 2-27-94, Formerly 17-160.300, Amended 3-24-96, 4-9-02, 6-8-04, 12-3-08, 7-30-14, 4-16-18.
Terms Used In Florida Regulations 62-160.300
- Contract: A legal written agreement that becomes binding when signed.
(b) For laboratories reporting data for drinking water compliance, certification shall be for all matrix/text method/analyte(s) combinations being reported.
(c) For the non-potable water matrix, laboratories shall apply for and receive DOH ELCP certification in at least one method for each analytical technology/analyte combination being measured. The Department will accept any of the combinations certified by the DOH ELCP, according to Fl. Admin. Code R. 64E-1.102, dated 1-24-05.
1. When a Department contract, order, permit or title 62 rules requires a specific method to be reported, laboratories shall report only that method. Laboratories may report additional analytes not published in the reported method, if the applicable requirements in Fl. Admin. Code R. 62-160.330 are met, and the laboratory is certified according to Fl. Admin. Code R. 62-160.300(1)(c)
2. Except as noted in subFl. Admin. Code R. 62-160.300(1)(c)1., above, laboratories may report results by any method that is equivalent in technology to the method for which they hold certification, provided they are certified according to Fl. Admin. Code R. 62-160.300(1)(c), for the analyte that is reported. When laboratories report a method for which they do not hold certification, the laboratory shall document that all requirements of the reported method are met.
3. If a laboratory is required to provide data for an analyte for which, according to subsection 62-160.320(1), F.A.C., no method is published for the non-potable water matrix, or the published method for the non-potable water matrix does not meet required data quality objectives established by the Department for a project, but a method is published for the drinking water matrix, and the Department has recognized that the published drinking water method meets the data quality objectives for the Department project for which the method will be used according to subsection 62-160.320(1), F.A.C., the laboratory is not required to obtain certification for the analytical technology/analyte combination in the non-potable water matrix. However, the laboratory must be certified in the drinking water matrix for the reported test method/analyte combination.
(d) For all other matrices, laboratories shall apply for and receive certification for all matrix/test method/analyte combinations that are reported to the Department.
(2) To the extent possible, a laboratory must be certified as specified in subsection 62-160.300(1), F.A.C., before reporting results for a given matrix/analytical technology or test method/analyte combination. However, if a laboratory makes a written request to the Department to use a method that is not certified, the Department will allow a laboratory to begin using a method before the certification process is complete if the following requirements are met.
(a) The laboratory must have met all the requirements for certification except for the on-site visit by DOH ELCP inspectors. The laboratory must be prepared to provide to the Department copies of the relevant application, applicable performance test sample results and the initial demonstration of capability.
(b) The precision, accuracy and method detection limits generated by the laboratory must meet or exceed the project specific data quality objectives.
(c) The laboratory shall notify the Department of the status of its certification application within 5 business days of receiving notification by DOH ELCP of the certification granted for the specific matrix/analytical technology or test method/analyte combination requested.
(3) Laboratory certification by the DOH ELCP is not required for the following test procedures identified in subsections 62-550.550(1) and (2), F.A.C., when conducted by an operator licensed under Fl. Admin. Code Chapter 62-602, or by persons under the direct supervision of a licensed operator, for the purposes of drinking water compliance:
(a) Alkalinity;
(b) Bromide;
(c) Calcium;
(d) Chlorite (only at entrances to distribution systems);
(e) Specific conductance;
(f) Disinfectant residual (includes residual chlorine);
(g) Orthophosphate;
(h) pH;
(i) Silica;
(j) Specific ultraviolet absorbance;
(k) Temperature;
(l) Total organic carbon;
(m) Turbidity, or
(n) Any analytes in addition to those listed in paragraphs 62-160.300(3)(a) through 62-160.300(3)(m), F.A.C., above that are exempted from laboratory certification according to subsections 62-550.550(1) and 62-550.550(2), F.A.C., for the specific compliance applications described therein.
(o) The analytes exempted in paragraphs 62-160.300(3)(a) through 62-160.300(3)(n), F.A.C., above shall be analyzed according to all applicable requirements for analyses according to subsections 62-550.550(1) and 62-550.550(2), F.A.C., for the specific compliance applications described therein.
(p) In cases where the Department has a specific field testing method standard operating procedure (e.g., FT 1100 for pH, in DEP-SOP-001/01, which is incorporated by reference in subFl. Admin. Code R. 62-160.800(1)(a)19.), the laboratory or authorized person, as described in Fl. Admin. Code R. 62-550.550, shall follow the Department’s procedures. For all other analytes, a laboratory or authorized person, as described in Fl. Admin. Code R. 62-550.550, shall only use test methods that are acceptable for drinking water compliance, as specified in Fl. Admin. Code R. 62-550.550 and shall follow all requirements for calibration verification according to DEP SOP FT 1000 in DEP-SOP-001/01, which is incorporated by reference in subFl. Admin. Code R. 62-160.800(1)(a)18.
(4) Certification by the DOH ELCP is not required when conducting the test procedures for the analytes listed in paragraphs 62-160.300(4)(a) through (h), F.A.C., because the Department’s standard operating procedures (SOPs) are more stringent than the corresponding laboratory test methods certified by DOH ELCP. When conducting these test procedures, laboratories shall follow the applicable SOPs in DEP-SOP-001/01 (January 2017), which are incorporated by reference in Fl. Admin. Code R. 62-160.800(1)(a)
(a) pH;
(b) Dissolved oxygen;
(c) Specific conductance;
(d) Temperature;
(e) Total residual chlorine (including free available chlorine);
(f) Salinity;
(g) Turbidity; and,
(h) Any other test with a specified holding time of fifteen minutes or less when performed as a field procedure.
(5) Certification is not required for the following tests or analyses:
(a) Any analyses related solely to internal process control, unless the test data are reported to the Department to meet compliance monitoring requirements for a Department-issued permit;
(b) Laboratory tests conducted for research projects, as described in Fl. Admin. Code R. 62-160.600, or
(c) Methods used by statutorily created volunteer monitoring organizations, when the Department has reviewed and concluded that the organization’s Standard Operating Procedures provide sufficient quality assurance requirements for Department purposes.
(6) Certification by the DOH ELCP is not required for methods and procedures required to perform the Specific Oxygen Uptake Rate (SOUR) test, when performed by an operator certified in accordance with Fl. Admin. Code Chapter 62-602, or persons under the direction of a certified operator, as authorized by Fl. Admin. Code Chapter 62-640
(7) Certification is not required for any test in which the reported result is a calculation from the results of other tests for which the laboratory holds certification by the DOH ELCP.
(8) Certification is not required for those matrix/method/analyte combinations (such as taxonomic identification) that are not included in the DOH ELCP scope of accreditation.
(9) If certification is not required (see subsections 62-160.300(3) through (8), F.A.C.), laboratory organizations shall follow the relevant Department-approved methods as provided in Fl. Admin. Code R. 62-160.320, and shall meet all other requirements for laboratories as provided in this chapter.
Rulemaking Authority 403.061, 403.0623, 403.0625, 403.863 FS. Law Implemented 373.026, 373.309, 373.409, 373.413, 373.414, 373.416, 373.4592, 376.303, 376.305, 376.3071, 403.0623, 403.0625, 403.087, 403.088, 403.0881, 403.504, 403.704, 403.707, 403.722, 403.803, 403.853 FS. History-New 1-1-91, Amended 2-4-93, 2-27-94, Formerly 17-160.300, Amended 3-24-96, 4-9-02, 6-8-04, 12-3-08, 7-30-14, 4-16-18.